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in 75 ml of acetonitrile. The mixture is allowed to stand at
-20 C for about 1.5 hours during which the suspended material dissolves, and the d-lysergic acid is
converted to the mixed anhydride of lysergic and trifluoroacetic acids. The mixed anhydride can be
separated in the form of an oil by evaporating the solvent in vacuo at a temperature below 0 C, but this
is not necessary. Everything must be kept anhydrous.
Step II. Use Yellow light
The solution of mixed anhydrides in acetonitrile from Step I is added to 150 ml of a second
solution of acetonitrile containing 7.6 g of diethylamide. The mixture is held in the dark at room
temperature for about 2 hours. The acetonitrile is evaporated in vacuo, leaving a residue of LSD-25
plus other impurities. The residue is dissolved in 150 ml of chloroform and 20 ml of ice water. The
chloroform layer is removed and the aqueous layer is extracted with several portions of chloroform. The
chloroform portions are combined and in turn washed with four 50 ml portions of ice-cold water. The
chloroform solution is then dried over anhydrous Na2SO4 and evaporated in vacuo.
This procedure gives good yield and is very fast with little iso-lysergic acid being formed (its
effect are mildly unpleasant). However, the stoichiometry must be exact or yields will drop.
Step I. Use White light
Sulphur trioxide is produced in anhydrous state by carefully decomposing anhydrous ferric
sulphate at approximately 480 C. Store under anhydrous conditions.
Step II. Use White light
A carefully dried 22 litre RB flask fitted with an ice bath, condenser, dropping funnel and
mechanical stirrer is charged with 10 to 11 litres of dimethylformamide (freshly distilled under reduced
pressure). The condenser and dropping funnel are both protected against atmospheric moisture. 2 lb of
sulphur trioxide (Sulfan B) are introduced drop wise, very cautiously stirring, during 4 to 5 hours. The
temperature is kept at 0-5 C throughout the addition. After the addition is complete, the mixture is
stirred for 1-2 hours until some separated, crystalline sulphur trioxide-dimethylformamide complex has
dissolved. The reagent is transferred to an air- tight automatic pipette for convenient dispensing, and
kept in the cold. Although the reagent, which is colourless, may change from yellow to red, its efficiency
remains unimpaired for three to four months in cold storage. An aliquot is dissolved in water and titrated
with standard NaOH to a phenolphthalein end point.
Step III. Use Red light
A solution of 7.15 g of d-lysergic acid mono hydrate (25 mmol) and 1.06 g of lithium hydroxide
hydrate (25 mmol) in 200 ml of MeOH is prepared. The solvent is distilled on the steam bath under
reduced pressure. the residue of glass-like lithium lysergate is dissolved in 400 ml of anhydrous dimethyl
formamide. From this solution about 200 ml of the dimethyl formamide is distilled off at 15 ml pressure
through a 12 inch helices pa
Mexico another species which he named LOPHOPHORA DIFFUSA. This plant is
yellow-green, soft, ribless and contains a somewhat different alkaloid mixture
with far less mescaline that L. williamsi.
About half an hour after ingesting the buttons the first effects are felt. There is a
feeling of strange intoxication and shifting consciousness with minor perceptual
changes. There may also be strong physical effects, including respiratory
pressure, muscle tension (especially face and neck muscles), and queasiness or
possible nausea. Any unpleasant sensations should disappear within an hour.
After this the state of altered consciousness begins to manifest itself. The
experience may vary with the individual, but among the possible occurences are
feelings of inner tranquillity, oneness with life, heightened awareness, and rapid
thought flow. During the next several hours these effects will deepen and
become more visual. Colors may become more intense. Halos and auras may
appear about things. Objects may seem larger, smaller , closer or more distant
than they actually are. Often persons will notice little or no changes in visual
perception while beholding the world about them, but upon closing their eyes
they will see on their mind-screen wildly colorful and constant changing patterns.
After several more hours the intensity of the experience gradually relaxes.
Thought becomes less rapid and diffuse and more ordered. In the Navajo peyote
ritual this change of thought flow is used wisely. During the first part of the
ceremony the participants submit to the feeling and let the peyote teach them.
During the latter part of the ritual the mind turns to thoughtful contemplation and
understanding with the conscious intellect what the peyote has taught the
The entire experience may last from 6 to 12 hours depending upon the individual
and the amount of the plant consumed. After all the peyote effects have passed
there is no comedown. One is likely to feel pleasantly relaxed and much a peace
with the world. Although there is usually no desire for food during the experience
one would probably have a wholesome appetite afterwards.
METHODS OF USE
The most common method of use is simply to chew up and swallow the fresh or
dried buttons after removing the tufts and sand. This is the way it is almost
always done at Indian ceremonies. Most people find the taste of this cactus
unbearably bitter. The Indians, however, feel if ones heart is pure, the bitterness
will not be tasted. Many have found that by not cringing from the taste, but rather
letting ones senses plunge directly to the center of the bitterness, a sort of
seperation from the offensive flavor is experienced. One is aware of the
bitterness, but it no longer disturbs him. This is similar to the practice of bringing
ones consciousness to the center of pain so that detachment may occur. It is not
a difficult trick, but it takes som
But in the early treatises on mushrooms, before von Strahlenbergs journey into
Siberia, we find no intoxicating properties attributed to the amanita muscaria.
It seems clear that cooking attenuates or kills the distinctive virtue of the fly
amanita. In Italy and France it is not rare to find individuals who habitually eat
this mushroom with impunity.
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